4-(4-Chlorophenyl)but-2-yn-1-ol → HCID 13660260, 화합물

HRID 464029노트

반응식

HRID 464029 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]#[C:10][CH2:11][OH:12])=[CH:4][CH:3]=1.[H][H]>CC(C)=O.[Pd].CC([O-])=O.CC([O-])=O.[Pb+2]>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8]/[CH:9]=[CH:10]\[CH2:11][OH:12])=[CH:6][CH:7]=1

참가 물질

5

반응물 2

HCID 136602584-(4-Chlorophenyl)but-2-yn-1-olHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 13660260HCID 13660260, 화합물

시약·촉매·용매 2

HCID 131709914Lindlars catalyst촉매HCID 180Acetone용매

실험 절차

Dissolve 10 g (0.055 mole) of 4-(4-chlorophenyl)but-2-yn-1-ol in 100 ml of acetone. Add 0.6 g of Lindlar's catalyst. Stir the mixture under 1 atmosphere of hydrogen at room temperature. Follow the progress of the reaction by NMR. At the completion of the reaction, filter to remove the catalyst and evaporate to yield the title compound.

후처리

  1. customthe progress of the reaction by NMR
  2. customAt the completion of the reaction
  3. filtrationfilter
  4. customto remove the catalyst
  5. customevaporate

출처 및 근거

ORD 기록
ord-e9db3053a42a47aca4797f058a311f27
출처 데이터셋
uspto-grants-1985_10
특허 번호
US04545995

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