참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | Chloromethyl ethyl ether | HCID 18523 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | (Ethoxymethyl)(triphenyl)phosphanium chloride | HCID 21470303 | — |
반응 단계
A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04173463 |
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| 출처 데이터셋 | uspto-grants-1979_11 |
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| ORD ID | ord-3204c8b2736246ee820e2cf7f1906092 |
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| 출처 메모 | uspto-grants-1979_11 |
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