참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Amino-2-methylbutyronitrile | HCID 15576830 | — |
| 촉매 | Hexadecyltrimethylammonium chloride | HCID 8154 | — |
| 생성물 | 2,2'-Azobis(2-methylbutyronitrile) | HCID 93079 | 173.8% |
반응 단계
The resulting aqueous dispersion of N,N-dichloro-2-amino-2-methylbutanenitrile was adjusted to pH7 by the addition of caustic soda and 3 ml of "Arquad 16-29%" surfactant added. After addition of a further 2.2 equivalents of caustic soda, 16.8 gm of 2-amino-2-methylbutanenitrile were added slowly over 60 minutes whilst maintaining the temperature at 20° C. The resulting suspension was filtered, washed and dried to yield 28.6 gm of the title compound (yield 84.2%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04546174 |
|---|
| 출처 데이터셋 | uspto-grants-1985_10 |
|---|
| ORD ID | ord-53d103c42b304bc9a113775e85116898 |
|---|
| 출처 메모 | uspto-grants-1985_10 |
|---|
