Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Octyloxy)benzoic acid → 4-Octyloxy-3-bromobenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-Octyloxy-3-bromobenzoic acid | HCID 23333447 | — |
반응 단계
A 25 g (0.1 mole) amount of p-octyloxybenzoic acid was suspended in 120 ml of water. The temperature was increased to between 50° C. and 55° C. and 17.6 g (0.11 mole) of bromine were added over a period of 7 hours at that temperature. The suspended solids were then filtered and recrystallized from ethanol and pure 4-octyloxy-3-bromobenzoic acid was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04173545 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-a3cd020d4ab04b65b1bc5990ffdfda26 |
| 출처 메모 | uspto-grants-1979_11 |