5-(4-Methoxyphenylazo)salicoyl chloride → HCID 178492410, 화합물

HRID 46425

반응식

HRID 46425 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]=[N:10][C:11]2[CH:19]=[C:15]([C:16](Cl)=[O:17])[C:14]([OH:20])=[CH:13][CH:12]=2)=[CH:5][CH:4]=1.[NH2:21][CH2:22][C:23]1[NH:27][N:26]=[N:25][N:24]=1>>[OH:20][C:14]1[CH:13]=[CH:12][C:11]([N:10]=[N:9][C:6]2[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)=[CH:19][C:15]=1[C:16]([NH:21][CH2:22][C:23]1[NH:27][N:26]=[N:25][N:24]=1)=[O:17]

참가 물질

3

반응물 2

HCID 1355740405-(4-Methoxyphenylazo)salicoyl chlorideHCID 178510704HCID 178510704, 화합물

생성물 1

HCID 178492410HCID 178492410, 화합물

실험 절차

5-(4-Methoxyphenylazo)salicoyl chloride and 5-aminomethyltetrazole were reacted together under the conditions described for the preparation of Dye 6 to form Dye 16, m.p. 220°-225° decomp., after crystallization from aqueous acetic acid, λmax (methanol)=350 nm.

후처리

  1. customdescribed for the preparation of Dye 6
  2. customto form Dye 16, m.p. 220°-225° decomp.
  3. customafter crystallization from aqueous acetic acid, λmax (methanol)=350 nm

출처 및 근거

ORD 기록
ord-ab442c581dba46a5b83e1ebc5e3da70f
출처 데이터셋
uspto-grants-1979_11
특허 번호
US04173478

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