Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Acetanilide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Phosphonium | HCID 5460504 | — |
| 생성물 | Acetanilide | HCID 904 | 20% |
반응 단계
To the same reaction mixture containing the phosphonium salt as in Example 1 was added a mixture of 3.0 g. (0.05 mole) of acetic acid and 5.2 g. (0.056 mole) of aniline, and the resulting mixture was reacted under reflux for 2 hours. Thereafter, the same aftertreatment as in Example 1 was effected to obtain acetanilide, yield 20% based on acetic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04173563 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-5125bfbe373845828fb7c1f366821596 |
| 출처 메모 | uspto-grants-1979_11 |