Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methane → HCID 13319896, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methane | HCID 297 | — |
| 반응물 | 3,4-Dihydro-6,7-dimethoxy-1-phenyl-3-(3-pyridyl)isoquinoline | HCID 13319895 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Diethylene glycol diethyl ether | HCID 8179 | — |
| 생성물 | HCID 13319896 | HCID 13319896 | 80.5% |
반응 단계
5.0 g of 3,4-dihydro-6,7-dimethoxy-1-phenyl-3-(3-pyridyl)isoquinoline in 150 ml of diethylene glycol diethyl ether are heated at 160° C. under an atmosphere of nitrogen with 2.5 g of palladium on animal charcoal (10%) for 2.5 hours. The catalyst is filtered off, the solution is evaporated in a rotary evaporator and the residue is washed with ether. 4.0 g of the isoquinoline compound of melting point 176°-177° C. are isolated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04547508 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-342258c5f3004a2e9040b94610ad1e0f |
| 출처 메모 | uspto-grants-1985_10 |