Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 13373474, 화합물 → 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-pyrid-4-ylmethylpyrimid-4-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 13373474 | HCID 13373474 | — |
| 반응물 | 2-[N-(3-aminopropyl)-N-benzylamino)pyridine | HCID 20150364 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-pyrid-4-ylmethylpyrimid-4-one | HCID 20262891 | — |
반응 단계
2-[N-(3-aminopropyl)-N-benzylamino)pyridine (1.0 g) and 2-nitroamino-5-(pyrid-4-ylmethyl)pyrimid-4-one (0.68 g) were heated together under reflux in pyridine (2.5 ml) for 23 hr. After stripping the residue was twice crystallized from ethanol/water to give 2-[3-(N-benzyl-N-pyrid-2-ylamino)propylamino]-5-pyrid-4-ylmethylpyrimid-4-one 1.6 H2O, 0.86 g (68%) m.p. 87°-89° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04547506 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-7ed901a7345a4bd2ba1887c458807b33 |
| 출처 메모 | uspto-grants-1985_10 |