참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methyl nadic anhydride | HCID 32802 | — |
| 촉매 | 2,5-Dimethyl-2,5-DI-(benzoylperoxy)hexane | HCID 75796 | — |
| 생성물 | Epoxy-styrene | HCID 14299145 | — |
반응 단계
To this inhibited epoxy diester-styrene mixture 5.49 parts of NADIC methyl anhydride and 0.048 part of 2,5-dimethyl-2,5 bis(benzoyl peroxy) hexane catalyst (sold by Wallace & Tiernan Inc. under the trade name of Luperox 118) were added, at 25° C., to provide the solventless epoxy-styrene impregnating varnish. The catalyst used has a catalytic reaction "kick off" temperature of about 115° C., i.e., it will have a definite catalytic effect to initiate a cure reaction at over about 115° C. The viscosity of the epoxy-styrene impregnating varnish was measured to be about 10 cps to 15 cps at 25° C. To this resin system 0.029 part of various metal acetylacetonates were added. One sample, containing no metal acetylacetonate was used as a control. The weight ratio of epoxy mixture: styrene: metal acetylacetonate was 1:1.9:0.0029. This varnish was prepared in 1 gallon laboratory batches and in 250 gallon large scale commercial batches.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04173593 |
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| 출처 데이터셋 | uspto-grants-1979_11 |
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| ORD ID | ord-74e2baf889884f59b7c28b7669ce62c6 |
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| 출처 메모 | uspto-grants-1979_11 |
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