Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl 3-(4-chlorophenyl)-2-propenoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-Propenoic acid, 3-(4-chlorophenyl)- | HCID 15371 | — |
| 생성물 | Methyl 3-(4-chlorophenyl)-2-propenoate | HCID 98955 | — |
반응 단계
A suspension of 300 g of 4-chlorocinnamic acid (J. Am. Chem. Soc., 89:3803, 1967) and 25 ml of concentrated sulfuric acid in 1.7 liters of methanol is heated to reflux for 24 hours. The solution is concentrated, and filtered to give as a white solid, p-chlorocinnamic acid methyl ester, mp 74°-5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04548947 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-bdc4760b50f9400fb595e7e11a867d3c |
| 출처 메모 | uspto-grants-1985_10 |