Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl chloroformate → HCID 13505629, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl chloroformate | HCID 10928 | — |
| 반응물 | 2-[(4-Methoxyphenyl)amino]benzoic acid | HCID 202918 | — |
| 생성물 | HCID 13505629 | HCID 13505629 | — |
반응 단계
A suspension of 40 g of 2-(4-methoxyphenylamino)benzoic acid in 200 ml of ethyl chloroformate was heated at reflux for 24 hours. The reaction mixture was cooled in an ice-bath and the solid which separated was collected by filtration to give 31 g of N-(4-methoxyphenyl)isatoic anhydride after 6 hours of drying in a vacuum oven. An additional 9 g of product was obtained by concentration of the filtrate in vacuo.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04549016 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-d2b9e70969cb481ba33f6ccc21c83996 |
| 출처 메모 | uspto-grants-1985_10 |