Trifop → HCID 13505617, 화합물

HRID 464912

반응식

HRID 464912 반응식
[F:1][C:2]([F:23])([F:22])[C:3]1[CH:21]=[CH:20][C:6]([O:7][C:8]2[CH:19]=[CH:18][C:11]([O:12][CH:13]([CH3:17])[C:14](O)=[O:15])=[CH:10][CH:9]=2)=[CH:5][CH:4]=1.[Cl:24][C:25]1[CH:30]=[CH:29][C:28]([Cl:31])=[CH:27][C:26]=1[S:32]([N:35]=C=O)(=[O:34])=[O:33]>>[Cl:24][C:25]1[CH:30]=[CH:29][C:28]([Cl:31])=[CH:27][C:26]=1[S:32]([NH:35][C:14](=[O:15])[CH:13]([O:12][C:11]1[CH:10]=[CH:9][C:8]([O:7][C:6]2[CH:20]=[CH:21][C:3]([C:2]([F:23])([F:1])[F:22])=[CH:4][CH:5]=2)=[CH:19][CH:18]=1)[CH3:17])(=[O:33])=[O:34]

참가 물질

3

반응물 2

HCID 181206TrifopHCID 128751872,5-Dichlorobenzene-1-sulfonyl isocyanate

생성물 1

HCID 13505617HCID 13505617, 화합물

실험 절차

A solution of one gram (0.0031 mole) 2-[4-(4-trifluoromethylphenoxy)phenoxy]-propionic acid in dry CHCH3 was treated with 0.8 gram (g) (0.0081 mole) 2,5-dichlorobenzene sulfonyl isocyanate. The solution was stirred for approximately 18 hours, then heated to reflux for three hours, followed by cooling.

후처리

  1. temperatureheated
  2. temperatureto reflux for three hours
  3. temperatureby cooling

출처 및 근거

ORD 기록
ord-1964ed97a263462cb25e4e9a6d4bd11f
출처 데이터셋
uspto-grants-1985_10
특허 번호
US04549901

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