Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl-(2-piperidin-2-yl-ethyl)-amine → 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl-(2-piperidin-2-yl-ethyl)-amine | HCID 296295 | — |
| 반응물 | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 13578559 | — |
반응 단계
The title compound is prepared analogously to Example 2 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 2-[2-(dimethylamino)ethyl]piperidine to give colorless crystals, mp. 155°-157° C. (acetonitrile).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04550107 |
| 출처 데이터셋 | uspto-grants-1985_10 |
| ORD ID | ord-60e390bd0a8b45b6a7d430164a616997 |
| 출처 메모 | uspto-grants-1985_10 |