Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isothiocyanic acid, p-dimethylaminophenyl ester → N-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethy](diphenylmethyl)amino]acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isothiocyanic acid, p-dimethylaminophenyl ester | HCID 75047 | — |
| 반응물 | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| 반응물 | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(2,2-diphenylethyl)amino]acetamide | HCID 19874997 | — |
| 생성물 | N-[2,6-bis(1-Methylethyl)phenyl]-2-[[[[4-(dimethylamino)phenyl]amino]thioxomethy](diphenylmethyl)amino]acetamide | HCID 86746182 | — |
반응 단계
When in the procedure of Example 80 an appropriate amount of 4-dimethylaminophenylisothiocyanate was substituted for ethyl isocyanato acetate and an appropriate amount of the product of Example 4 was substituted for the product of Example 70 and the general procedure of Example 80 was followed the title compound was obtained. Total yield, 0.38 g (33%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05153226 |
| 출처 데이터셋 | uspto-grants-1992_10 |
| ORD ID | ord-d1ae2efd19294a3f888d5f51c5dcd1a9 |
| 출처 메모 | uspto-grants-1992_10 |