Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Bromooctadecane → 3,5-Dioctadecyloxybenzoic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Bromooctadecane | HCID 8218 | — |
| 반응물 | Benzoic acid, 3,5-dihydroxy-, ethyl ester | HCID 20098 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3,5-Dioctadecyloxybenzoic acid ethyl ester | HCID 53731475 | — |
반응 단계
50 m mol of 3,5-dihydroxybenzoic acid ethyl ester, 120 m mol of stearyl bromide, and 110 m mol of sodium were made to react in ethanol, thereby forming 35 m mol of 3,5-dioctadecyloxybenzoic acid ethyl ester. This ester, 25 m mol, was first hydrolyzed into the corresponding acid, which in turn was converted into its acid chloride. The acid chloride was reacted in the same way as in Example 1, whereby 10 m mol of N-(3,5-dioctadecyloxybenzoyl)-N'methylsulfonyl-p-quinonediimine was obtained which is represented by the following formula: ##STR30##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05153680 |
| 출처 데이터셋 | uspto-grants-1992_10 |
| ORD ID | ord-0708f62d736c4ba789917a02358715dc |
| 출처 메모 | uspto-grants-1992_10 |