Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4,5-Trimethoxybenzaldehyde → N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| 반응물 | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine | HCID 20386241 | 94% |
반응 단계
Interaction of 21 g of 3,4,5-trimethoxybenzaldehyde with 11 g of 3-dimethylaminopropylamine in 80 ml. of benzene following the procedure described in Example 1 yields 28.2 g of product as an oil, boiling point 162°-167° C. at 0.4-0.5 mm. of Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04174317 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-4b3cc334fad24d0e82410294c773b13e |
| 출처 메모 | uspto-grants-1979_11 |