Benzyl 3-chlorocarbonylbenzoate → 4-(3-Benzyloxycarbonylbenzoyloxy)-2-pyridone

HRID 466115노트

반응식

HRID 466115 반응식
[OH:1][C:2]1[CH:7]=[CH:6][NH:5][C:4](=[O:8])[CH:3]=1.[CH2:9]([O:16][C:17]([C:19]1[CH:20]=[C:21]([CH:25]=[CH:26][CH:27]=1)[C:22](Cl)=[O:23])=[O:18])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[CH2:9]([O:16][C:17]([C:19]1[CH:20]=[C:21]([CH:25]=[CH:26][CH:27]=1)[C:22]([O:1][C:2]1[CH:7]=[CH:6][NH:5][C:4](=[O:8])[CH:3]=1)=[O:23])=[O:18])[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

참가 물질

3

반응물 2

HCID 19815207Benzyl 3-chlorocarbonylbenzoateHCID 546960044-Hydroxy-2(1H)-pyridinone

생성물 1

HCID 140496634-(3-Benzyloxycarbonylbenzoyloxy)-2-pyridone수율 49%

실험 절차

The general procedure of Example 1 was repeated using 2.80 g of 4-hydroxy-2-pyridone and 14.70 g of 3-benzyloxycarbonylbenzoyl chloride, thereby producing 4.29 g of the title compound in a yield of 49%.

출처 및 근거

ORD 기록
ord-cb2922094a564731a4ed5320f3c5aef5
출처 데이터셋
uspto-grants-1992_10
특허 번호
US05155113

반응 노트

불러오는 중…