Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 5-Aminoacenaphthene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Acenaphthene | HCID 6734 | — |
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | 5-Nitroacenaphthene | HCID 11769 | — |
| 반응물 | Tin atom | HCID 5352426 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-Aminoacenaphthene | HCID 62547 | — |
반응 단계
5-Nitroacenaphthene is made by nitrating acenaphthene with nitric acid in the presence of acetic acid according to the method of Rowe and Davies, J. Chem. Soc. 117, 1346 (1920). Standard reduction methods using tin or stannous chloride in hydrochloric acid or by using Raney nickel with ethanol or hydrazine produces 5-aminoacenaphthene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04174342 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-1a06f9ffbc2c46afaf47b657be09d7f6 |
| 출처 메모 | uspto-grants-1979_11 |