2-Methylbenzoyl chloride → HCID 178424297, 화합물

HRID 466131노트

반응식

HRID 466131 반응식
C[Si](C)(C)[O:3][C:4]1[CH:9]=[C:8]([O:10][Si](C)(C)C)[CH:7]=[CH:6][N:5]=1.[CH3:17][C:18]1[CH:26]=[CH:25][CH:24]=[CH:23][C:19]=1[C:20](Cl)=[O:21]>>[OH:10][C:8]1[CH:7]=[CH:6][N:5]=[C:4]([O:3][C:20](=[O:21])[C:19]2[CH:23]=[CH:24][CH:25]=[CH:26][C:18]=2[CH3:17])[CH:9]=1

참가 물질

3

반응물 2

HCID 702762-Methylbenzoyl chlorideHCID 21819823HCID 21819823, 화합물

생성물 1

HCID 178424297HCID 178424297, 화합물수율 44.3%

실험 절차

The general procedure of Example 27 was followed using 4.0 g of 2,4-bis(trimethylsilyloxy)-pyridine and 2.92 g of 2-methylbenzoyl chloride, thereby producing 1.59 g of the title compound in a yield of 44.18%.

출처 및 근거

ORD 기록
ord-7040f849d4e74d7f9dce179ed8717aba
출처 데이터셋
uspto-grants-1992_10
특허 번호
US05155113

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