Valeryl chloride → 2-Oxo-1,2-dihydropyridin-4-yl pentanoate

HRID 466148노트

반응식

HRID 466148 반응식
C[Si](C)(C)[O:3][C:4]1[CH:9]=[C:8]([O:10][Si](C)(C)C)[CH:7]=[CH:6][N:5]=1.[C:17](Cl)(=[O:22])[CH2:18][CH2:19][CH2:20][CH3:21]>>[C:17]([O:10][C:8]1[CH:7]=[CH:6][NH:5][C:4](=[O:3])[CH:9]=1)(=[O:22])[CH2:18][CH2:19][CH2:20][CH3:21]

참가 물질

3

반응물 2

HCID 61186Valeryl chlorideHCID 21819823HCID 21819823, 화합물

생성물 1

HCID 140496732-Oxo-1,2-dihydropyridin-4-yl pentanoate수율 41%

실험 절차

The general procedure of Example 31 was followed using 1.00 g of 2,4-bis(trimethylsilyloxy)-pyridine and 1.02 ml of n-pentanoyl chloride, thereby giving 310 mg of the title compound in a yield of 41%.

출처 및 근거

ORD 기록
ord-282cad0db983439c9fb5d99ce8a06871
출처 데이터셋
uspto-grants-1992_10
특허 번호
US05155113

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