3-Methylbenzoyl chloride → 3-Cyano-6-(3-methylbenzoyloxy)-2-hydroxypyridine

HRID 466167노트

반응식

HRID 466167 반응식
[C:1]([C:3]1[C:4]([OH:10])=[N:5][C:6]([OH:9])=[CH:7][CH:8]=1)#[N:2].[CH3:11][C:12]1[CH:13]=[C:14]([CH:18]=[CH:19][CH:20]=1)[C:15](Cl)=[O:16]>>[C:1]([C:3]1[C:4]([OH:10])=[N:5][C:6]([O:9][C:15](=[O:16])[C:14]2[CH:18]=[CH:19][CH:20]=[C:12]([CH3:11])[CH:13]=2)=[CH:7][CH:8]=1)#[N:2]

참가 물질

3

반응물 2

HCID 743753-Methylbenzoyl chlorideHCID 178510101HCID 178510101, 화합물

생성물 1

HCID 1784253153-Cyano-6-(3-methylbenzoyloxy)-2-hydroxypyridine수율 58%

실험 절차

The general procedure of Example 81 was followed using 2.00 g of 3-cyano-2,6-dihydroxypyridine and 2.27 g of 3-methylbenzoyl chloride, thereby producing 2.16 g of the title compound in a yield of 58%.

출처 및 근거

ORD 기록
ord-a9564cf7c9d9482995ee40ba7964fca6
출처 데이터셋
uspto-grants-1992_10
특허 번호
US05155113

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