Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 5-Phenyl-2-trityltetrazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Trityl chloride | HCID 6456 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | HCID 178418369 | HCID 178418369 | — |
| 용매 | Acetone | HCID 180 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 5-Phenyl-2-trityltetrazole | HCID 3292959 | 100.7% |
반응 단계
To a suspension of 5-phenyltetrazole (5 g; 34 mmole), stirring in 55 mL of acetone, was added 3.6 g of triethylamine (36 mmoles). The mixture was aged for 15 minutes after which triphenylmethylchloride (10.0 g; 36 mmoles) in 20 mL of THF was added; the temperature rose 8°-10° C. After stirring for 1 hour, 75 mL of H2O was added and the mixture stirred for 1 hour. After filtration, washing with water and drying in vacuo at 70° C., 13.3 g of 18a was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05157040 |
| 출처 데이터셋 | uspto-grants-1992_10 |
| ORD ID | ord-47d3016f67464ec7b2cbdc3d2cc81882 |
| 출처 메모 | uspto-grants-1992_10 |