Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propylene Oxide → N-Chlorophthalimide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propylene Oxide | HCID 6378 | — |
| 반응물 | Phthalimide | HCID 6809 | — |
| 반응물 | Chlorine | HCID 24526 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-Chlorophthalimide | HCID 18997 | — |
반응 단계
To 150 ml. of dry methylene chloride were added 7.35 g. (0.05 mole) of phthalimide followed by 17.5 ml. (5 equiv.) of propylene oxide and 0.065 g. (0.5 mmoles) of diisopropylethylamine. The mixture was cooled to 0° C. and saturated with chlorine. The mixture was stirred for about 24 hours to provide approximately 50% conversion to N-chlorophthalimide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04175082 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-30bcf861e6db4b1091088b181ae54e82 |
| 출처 메모 | uspto-grants-1979_11 |