Benzaldehyde → Cyano(phenyl)methyl 2-methylpropanoate
반응식
[C:1]([O:6][C:7](=[O:11])[CH:8]([CH3:10])[CH3:9])(=O)[CH:2]([CH3:4])[CH3:3].[CH:12](=O)[C:13]1[CH:18]=CC=CC=1.[C-:20]#[N:21].[Na+]>O>[C:7]([O:6][CH:1]([C:20]#[N:21])[C:2]1[CH:4]=[CH:18][CH:13]=[CH:12][CH:3]=1)(=[O:11])[CH:8]([CH3:10])[CH3:9]참가 물질
5
반응 조건
- 온도
- 25 °C
실험 절차
A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).
후처리
- customA 100-ml round-bottomed flask equipped with a magnetic stirrer
- customThe mixture formed
출처 및 근거
- ORD 기록
- ord-b8b0d7af08bb45c5b88e08b5a8efd0a7
- 출처 데이터셋
- uspto-grants-1979_11
- 특허 번호
- US04175094
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