Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178421680, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Thiocarbohydrazide | HCID 2724189 | — |
| 반응물 | (1-Methylcyclopropyl)-glyoxylic acid tert-butylamide | HCID 20385839 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178421680 | HCID 178421680 | — |
반응 단계
183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04175188 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-e471648b4ae44be4b25f0eae45b4618f |
| 출처 메모 | uspto-grants-1979_11 |