참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | 2-Methyl-3-buten-2-ol | HCID 8257 | — |
| 반응물 | 2-Bromopropene | HCID 11202 | — |
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 촉매 | palladium(II) acetate | HCID 167845 | — |
| 생성물 | 2,5-Dimethyl-6-piperidinohex-4-en-2-ol | HCID 54073601 | 80% |
반응 단계
A mixture of 10 mmoles 2-bromopropene, 12.5 mmoles 2-methyl-3-buten-2-ol, 30 mmoles piperidine, 0.10 mmole palladium acetate and 0.20 mmole triphenylphosphine were heated together at 100° C. for 20 hrs. From the reaction mixture there was isolated an 80% yield of 2,5-dimethyl-6-piperidinohex-4-en-2-ol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04175187 |
|---|
| 출처 데이터셋 | uspto-grants-1979_11 |
|---|
| ORD ID | ord-36b3dc7de3a744b7b84c6924ec4ae3cb |
|---|
| 출처 메모 | uspto-grants-1979_11 |
|---|
