참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Dimethylacetamide | HCID 31374 | — |
| 반응물 | 1-Fluoro-5-methyl-2,4-dinitrobenzene | HCID 520705 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine | HCID 15022335 | 63% |
반응 단계
A mixture of 1-fluoro-5-methyl-2,4-dinitro-benzene (10 g, 50 mmol), DMA (12 g, 100 mmol) and DMF (50 nit) was heated at 100° C. for 4 h. The solution was cooled and poured into water. The precipitated red solid was collected, washed with water, and dried to give (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine (8.0 g, 63%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08623905B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_01 |
|---|
| ORD ID | ord-b8df435da39b42fd8e4410c5ca578235 |
|---|
| 출처 메모 | uspto-grants-2014_01 |
|---|
