Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Amino-1-propanol → 3-[(2-Chloro-6-nitrophenyl)amino]-1-propanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Amino-1-propanol | HCID 9086 | — |
| 반응물 | 2,3-Dichloronitrobenzene | HCID 18555 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | 3-[(2-Chloro-6-nitrophenyl)amino]-1-propanol | HCID 20385566 | — |
반응 단계
A mixture of 100 parts of 1,2-dichloro-3-nitrobenzene, 95 parts of 3-amino-1-propanol and 200 parts of butanol is stirred and refluxed overnight. The reaction mixture is cooled and evaporated. The residue is taken up in water and the product is extracted with methylbenzene. The extract is washed with water, dried, filtered and evaporated, yielding 115 parts of 3-[(2-chloro-6-nitrophenyl)amino]-1-propanol as a residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04175129 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-3cf7f60be5d04e27a25f57e8e5833753 |
| 출처 메모 | uspto-grants-1979_11 |