Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,6-Diiodohexane → 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione}
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,6-Diiodohexane | HCID 12373 | — |
| 반응물 | 1,1'-Butane-1,4-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763837 | — |
| 생성물 | 1,1'-Hexane-1,6-diylbis{5,5-dimethyl-3-[4-nitro-3-(trifluoromethyl)phenyl]imidazolidine-2,4-dione} | HCID 49763838 | 27% |
반응 단계
The experimental protocol used is the same as that described for the synthesis of the compound of Example 1, 1,6-diiodohexane replacing 1,4-dibromobutane. The expected compound is obtained in the form of a light yellow solid with a yield of 27%. Melting point: 187-188° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08624037B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-3ea8d0c5a6b24f7daeb679b1c6c2cb68 |
| 출처 메모 | uspto-grants-2014_01 |