Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3,5-Triiodobenzoic acid → (3,5-Diiodophenyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3,5-Triiodobenzoic acid | HCID 6948 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 생성물 | (3,5-Diiodophenyl)methanol | HCID 12330868 | — |
반응 단계
Using the procedure of B, Gaux and D. LeHenaff, Bull. Soc. Chem. Fr., 34, 505 (1974), 2,3,5-triiodobenzoic acid (Aldrich) was treated with lithium aluminum hydride to give 3,5-diiodobenzyl alcohol with m.p. of 136.5°-140° (literature 137°). Using the procedure outlined in Example 4, 3,5-diiodobenzyl alcohol was treated with n-hexyl chloroformate giving s in Table I (ND25 =1.5800).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04175544 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-f4c91a5d5e8b43e7a55dc8f6e8b0d5ec |
| 출처 메모 | uspto-grants-1979_11 |