Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetonitrile → 5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetonitrile | HCID 6342 | — |
| 반응물 | 4-Fluorophenol | HCID 9732 | — |
| 반응물 | 1-Methylcyclohexanol | HCID 11550 | — |
| 생성물 | 5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol | HCID 57470221 | — |
반응 단계
5-Amino-4-fluoro-2-(1-methylcyclohexyl)phenol (C-13) was synthesized following the general scheme above starting from 4-fluorophenol and 1-methylcyclohexanol. Overall yield (3%). HPLC ret. time 3.00 min, 10-99% CH3CN, 5 min run; ESI-MS 224.2 m/z (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08629162B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-c5b54898655047e1a040608c0831fa79 |
| 출처 메모 | uspto-grants-2014_01 |