Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 4-Chloro-2-fluoroaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 4'-Chloro-2'-fluoroacetanilide | HCID 853174 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Chloro-2-fluoroaniline | HCID 93898 | — |
반응 단계
A mixture of 119 parts of 4'-chloro-2'-fluoroacetanilide in 475 parts of ethanol and 200 parts of 37% hydrochloric acid was refluxed for 17 hours and the solvent removed at a reduced pressure of 300 mm.Hg to yield the moist, solid hydrochloride salt of 4-chloro-2-fluoroaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04175948 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-ebdbfc73549c44b5b2abb8ac1aa4e104 |
| 출처 메모 | uspto-grants-1979_11 |