5-Nitro-2-propoxyaniline → 2,4-Diaminopropoxybenzene
반응식
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([O:11][CH2:12][CH2:13][CH3:14])=[C:8]([NH2:10])[CH:9]=1)([O-])=O>CC#N>[CH2:12]([O:11][C:7]1[CH:6]=[CH:5][C:4]([NH2:1])=[CH:9][C:8]=1[NH2:10])[CH2:13][CH3:14]참가 물질
3
실험 절차
4-Propoxybenzene-1,3-diamine (D-5) was synthesized following the general scheme above starting from 5-nitro-2-propoxy-phenylamine. Yield (79%). HPLC ret. time 0.54 min, 10-99% CH3CN, 5 min run; ESI-MS 167.5 m/z (MH+).
후처리
- customYield (79%)
출처 및 근거
- ORD 기록
- ord-5783da88d20f4bdeb4abd90186ede14b
- 출처 데이터셋
- uspto-grants-2014_01
- 특허 번호
- US08629162B2
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