Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 2-Methylpyridine-3-carbonitrile | HCID 4738308 | — |
| 생성물 | N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine | HCID 54435625 | — |
반응 단계
N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared using the procedure of 4 A from 2-methyl-3-cyanopyridine (9.0 g, 0.076 m), DMF acetal (11.0 g, 0.092 m) and DMF (50 mL) yielding N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine b.p.=133°-135° (0.3 mm), m.p.=49°-50° after sublimation at 50° (0.3 mm).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04176183 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-4a2635ef6c464657ae9922b89defc428 |
| 출처 메모 | uspto-grants-1979_11 |