Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 5,6-Dimethoxy-3[4(3,4-dimethoxyphenyl)piperazino]methylene oxindole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 1-(3,4-Dimethoxyphenyl)piperazine | HCID 2736207 | — |
| 반응물 | HCID 178486553 | HCID 178486553 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5,6-Dimethoxy-3[4(3,4-dimethoxyphenyl)piperazino]methylene oxindole | HCID 54275679 | — |
반응 단계
3.00 g. of 5,6-Dimethoxy-3-hydroxymethylene oxindole, 2.3 g. acetic acid and 4.1 g. N-(3,4-dimethoxyphenyl)piperazine [J. Med. Chem. 10 (5) 812 (1967)] in 40 ml. benzene were reacted as described in Example 5 to give 4.67 g. product, m.p. 193°-195° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04176191 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-aa565e80a5ba49e980cf4d5fcfe8b3b1 |
| 출처 메모 | uspto-grants-1979_11 |