Acetic Acid → HCID 178490301, 화합물

HRID 47075

반응식

HRID 47075 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][C:11]=1[O:12][CH3:13])[NH:8][C:7](=[O:14])[C:6]2=[CH:15]O.[CH3:17][O:18][C:19]1[CH:20]=[C:21]([CH2:27][CH2:28][NH2:29])[CH:22]=[CH:23][C:24]=1[O:25][CH3:26].C(O)(=O)C>C1C=CC=CC=1>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:9](=[CH:10][C:11]=1[O:12][CH3:13])[NH:8][C:7](=[O:14])[C:6]2=[CH:15][NH:29][CH2:28][CH2:27][C:21]1[CH:22]=[CH:23][C:24]([O:25][CH3:26])=[C:19]([O:18][CH3:17])[CH:20]=1

참가 물질

5

반응물 3

HCID 176Acetic AcidHCID 8421HomoveratrylamineHCID 178486553HCID 178486553, 화합물

생성물 1

HCID 178490301HCID 178490301, 화합물

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

5.00 g. of 5,6-Dimethoxy-3-hydroxymethylene oxindole, 6.00 g. of 2(3,4-dimethoxyphenyl)ethylamine and 2.20 acetic acid in 40 ml. benzene was reacted as described in Example 5 to give 6.30 g. product, m.p. 164°-166° C.

후처리

  1. customto give 6.30 g

출처 및 근거

ORD 기록
ord-d59da3bc0c2c42b883b835031853d03e
출처 데이터셋
uspto-grants-1979_11
특허 번호
US04176191

연결된 노트

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