Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 3-[[(3,4-dimethoxyphenyl)methylamino]methylidene]-5,6-dimethoxy-1H-indol-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Veratrylamine | HCID 79832 | — |
| 반응물 | HCID 178486553 | HCID 178486553 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 3-[[(3,4-dimethoxyphenyl)methylamino]methylidene]-5,6-dimethoxy-1H-indol-2-one | HCID 178491076 | — |
반응 단계
5.00 g. of 5,6-Dimethoxy-3-hydroxymethylene oxindole, 6.00 g. of 3,4-dimethoxy benzylamine and 2.20 g. of acetic acid in 40 ml. benzene were reacted as described in Example 5 to give 5.44 g. of product, m.p. 198°-200° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04176191 |
| 출처 데이터셋 | uspto-grants-1979_11 |
| ORD ID | ord-097da2f5504447ae984f864cc7fdd477 |
| 출처 메모 | uspto-grants-1979_11 |