Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Ethylpyridin-2-amine → 4-Ethyl-5-iodopyridin-2-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Ethylpyridin-2-amine | HCID 118425 | — |
| 반응물 | N-Iodosuccinimide | HCID 120273 | — |
| 생성물 | 4-Ethyl-5-iodopyridin-2-amine | HCID 58200578 | — |
반응 단계
The title compound is synthesized according to general procedure GP1 starting from 5.0 g (41 mmol) 4-ethyl-pyridin-2-ylamine and 9.2 g (41 mmol) NIS. Yield after precipitation from the reaction mixture and isolation of additional product from the mother liquid by chromatography using silica gel: 10.3 g (100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633183B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-2c7b77c81fe6431e91dfa4bc4768f366 |
| 출처 메모 | uspto-grants-2014_01 |