Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorosulfamic acid → N-(2-Cyano-5-trifluoromethylphenyl)sulfamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorosulfamic acid | HCID 24499 | — |
| 반응물 | 2-Amino-4-(trifluoromethyl)benzonitrile | HCID 13439028 | — |
| 생성물 | N-(2-Cyano-5-trifluoromethylphenyl)sulfamide | HCID 67400577 | — |
반응 단계
Prepared as in Example 77a from 2-amino-4-trifluoromethylbenzonitrile and sulfamoyl chloride. 1H NMR (400 MHz, DMSO-d6) δ 7.53 (s, 1H), 7.74-7.76 (d, J=8.4 Hz, 1H), 8.01-8.03 (dd, J=8.4 Hz, 1.6 Hz, 1H), 8.23 (s, 1H), 10.16 (b, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-9956505b979f4670b5ed1ada39798555 |
| 출처 메모 | uspto-grants-2014_01 |