Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxybenzyl alcohol → 2-Nitro-6-(2-methoxybenzyloxy)benzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxybenzyl alcohol | HCID 69154 | — |
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 생성물 | 2-Nitro-6-(2-methoxybenzyloxy)benzonitrile | HCID 66746302 | 58% |
반응 단계
Prepared as in Example 111c from 2,6-dinitrobenzonitrile and 2-methoxybenzyl alcohol in 58% yield. 1H NMR (400 MHz, DMSO) δ 3.82 (s, 3H), 5.34 (s, 2H), 6.99 (t, J=7.6 Hz, 1H), 7.08 (d, J=8.4 Hz, 1H), 7.37 (t, J=8.4 Hz, 1H), 7.46 (d, J=6.0 Hz, 1H), 7.81 (d, J=7.6 Hz, 1H), 7.93-7.87 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-245d3f500d9441b2bf5db76eb9258306 |
| 출처 메모 | uspto-grants-2014_01 |