Methoxymethylbutanol → 2-(3-Methoxy-3-methylbutoxy)-6-nitrobenzonitrile

HRID 471698

반응식

HRID 471698 반응식
[CH3:1][O:2][C:3]([CH3:8])([CH3:7])[CH2:4][CH2:5][OH:6].[N+:9]([C:12]1[CH:19]=[CH:18][CH:17]=[C:16]([N+]([O-])=O)[C:13]=1[C:14]#[N:15])([O-:11])=[O:10]>>[CH3:1][O:2][C:3]([CH3:8])([CH3:7])[CH2:4][CH2:5][O:6][C:16]1[CH:17]=[CH:18][CH:19]=[C:12]([N+:9]([O-:11])=[O:10])[C:13]=1[C:14]#[N:15]

참가 물질

3

반응물 2

HCID 62118MethoxymethylbutanolHCID 520718Dinitrobenzonitrile

생성물 1

HCID 674011512-(3-Methoxy-3-methylbutoxy)-6-nitrobenzonitrile수율 52%

실험 절차

Prepared as in Example 215c from 3-methoxy-3-methylbutan-1-ol and 2,6-dinitrobenzonitrile in 52% yield. MS 265 (MH+).

출처 및 근거

ORD 기록
ord-4f75fd2ca6b24187b86c979287659b75
출처 데이터셋
uspto-grants-2014_01
특허 번호
US08633186B2

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