Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Prenderol → 2-(2-Ethyl-2-(hydroxymethyl)butoxy)-6-nitrobenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Prenderol | HCID 8284 | — |
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 생성물 | 2-(2-Ethyl-2-(hydroxymethyl)butoxy)-6-nitrobenzonitrile | HCID 67399880 | 86% |
반응 단계
Prepared as in Example 215c from 2,2-diethylpropane-1,3-diol and 2,6-dinitrobenzonitrile in 86% yield. 1H NMR (400 MHz, DMSO-d6) δ 0.80 (t, J=7.6 Hz, 6H), 1.34 (q, J=7.6 Hz, 4H), 3.33 (d, J=5.6 Hz, 2H), 3.96 (s, 2H), 4.57 (t, J=5.2 Hz, 1H), 7.74-7.76 (m, 1H), 7.84-7.90 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-8cea73de2f8e4e7ab69a0f014b5b3edd |
| 출처 메모 | uspto-grants-2014_01 |