Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dinitrobenzonitrile → Tert-butyl 4-(2-cyano-3-nitrophenoxy)butylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dinitrobenzonitrile | HCID 520718 | — |
| 반응물 | tert-Butyl N-(4-hydroxybutyl)carbamate | HCID 545141 | — |
| 생성물 | Tert-butyl 4-(2-cyano-3-nitrophenoxy)butylcarbamate | HCID 66665900 | 7% |
반응 단계
Prepared as in Example 215c from tert-butyl 4-hydroxybutylcarbamate and 2,6-dinitrobenzonitrile in 7% yield as a pale yellow solid. 1H NMR (400 MHz, DMSO-d6) δ 1.35 (s, 9H), 1.52-1.55 (m, 2H), 1.72-1.76 (m, 2H), 2.94-2.99 (m, 2H), 4.24 (t, J=6.8 Hz, 2H), 6.86 (brs, 1H), 7.69-7.72 (m, 1H), 7.85-7.90 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08633186B2 |
| 출처 데이터셋 | uspto-grants-2014_01 |
| ORD ID | ord-869e344172e04172aae62636868ef67d |
| 출처 메모 | uspto-grants-2014_01 |