2,2,4-Trimethyl-1,3-pentanediol → 2-(3-Hydroxy-2,2,4-trimethylpentyloxy)-6-nitrobenzonitrile

HRID 471739

반응식

HRID 471739 반응식
[CH3:1][C:2]([CH3:10])([CH:5]([OH:9])[CH:6]([CH3:8])[CH3:7])[CH2:3][OH:4].[N+:11]([C:14]1[CH:21]=[CH:20][CH:19]=[C:18]([N+]([O-])=O)[C:15]=1[C:16]#[N:17])([O-:13])=[O:12]>>[OH:9][CH:5]([CH:6]([CH3:8])[CH3:7])[C:2]([CH3:10])([CH3:1])[CH2:3][O:4][C:18]1[CH:19]=[CH:20][CH:21]=[C:14]([N+:11]([O-:13])=[O:12])[C:15]=1[C:16]#[N:17]

참가 물질

3

반응물 2

HCID 89462,2,4-Trimethyl-1,3-pentanediolHCID 520718Dinitrobenzonitrile

생성물 1

HCID 673992382-(3-Hydroxy-2,2,4-trimethylpentyloxy)-6-nitrobenzonitrile수율 90%

실험 절차

Prepared as in Example 215c from 2,2,4-trimethylpentane-1,3-diol and 2,6-dinitrobenzonitrile in 90% yield. MS 293 (MH+).

출처 및 근거

ORD 기록
ord-e468c37b4e2544daa55e686d79c5f845
출처 데이터셋
uspto-grants-2014_01
특허 번호
US08633186B2

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