Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 9,9'-Bianthryl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Anthrone | HCID 7018 | — |
| 촉매 | Zinc | HCID 23994 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 9,9'-Bianthryl | HCID 66105 | — |
반응 단계
After hydrochloric acid was added to an acetic acid solution of anthrone, it was refluxed upon addition of zinc. Thereafter it was refined in accordance with an ordinary method to obtain 9,9′-bianthryl. After it was added little by little to a melt of aluminum chloride and sodium chloride, the reaction mixture was poured into diluted hydrochloric acid and a solids constituent was collected. The solids constituent thus obtained was refined in accordance with an ordinary method to obtain target dibenzo[a,o]perylene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06699594B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-09a1edf32dea46fb8b70e9767bbae5d4 |
| 출처 메모 | uspto-grants-2004_03 |