Ethylamine → HCID 12715772, 화합물
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[N+:1]([C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:5]=1[C:6]#[N:7])([O-])=O.[CH2:15](N)[CH3:16]>C1COCC1>[CH2:15]([NH:1][C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([N+:12]([O-:14])=[O:13])[C:5]=1[C:6]#[N:7])[CH3:16]참가 물질
4
실험 절차
Prepared as in Example 90c from 2,6-dinitrobenzonitrile and a 2M ethylamine solution in THF in 88% yield. 1H NMR (400 MHz, DMSO-d6) δ 1.13 (t, J=7.6 Hz, 3H), 3.26-3.33 (m, 2H), 6.59 (bt, J=5.2 Hz, NH), 7.22 (d, J=9.2 Hz, 1H), 7.42 (d, J=8.0 Hz, 1H), 7.60 (t, J=8.4 Hz, 1H). MS 162 (M-Et).
출처 및 근거
- ORD 기록
- ord-3fad40cbeedc461682545241127ea0d0
- 출처 데이터셋
- uspto-grants-2014_01
- 특허 번호
- US08633186B2
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