Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → [2-(1-Methyl-pyrrolidin-yl)ethyl] thiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | 2-(2-Isothiocyanatoethyl)-1-methylpyrrolidine | HCID 21992328 | — |
| 생성물 | [2-(1-Methyl-pyrrolidin-yl)ethyl] thiourea | HCID 21992305 | — |
반응 단계
The 2-(2-isothiocyanatoethyl)-1-methylpyrrolidine and concentrated ammonium hydroxide (3 mL) were heated at 100° C. for 30 minutes. Additional ammonium hydroxide (1 mL) was added and heating was continued for an additional 30 minutes. The reaction mixture was allowed to cool to room temperature and then it was lyophilized to give [2-(1-methylpyrrolidin-2-yl)ethyl]thiourea as a very viscous colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06699866B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-b966538370894aab817f4a3432f2391f |
| 출처 메모 | uspto-grants-2004_03 |