Carbon Dioxide → Benzeneacetic acid, 4-bromo-

HRID 472952노트

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HRID 472952 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8](C(O)=O)[C:9]([OH:11])=[O:10])=[CH:4][CH:3]=1.C(=O)=O>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][C:9]([OH:11])=[O:10])=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 280Carbon DioxideHCID 21866616Propanedioic acid, 2-(4-bromophenyl)-

생성물 1

HCID 74654Benzeneacetic acid, 4-bromo-수율 1,099.1%

실험 절차

2-(4-Bromophenyl)malonic acid (36 g, 11 mmol) was heated at 165° C. until evolution of CO2. the production was crystallized from petrol ether to give 2-(4-bromophenyl)acetic acid (26 g, 87%).

후처리

  1. customthe production was crystallized from petrol ether

출처 및 근거

ORD 기록
ord-0c71970627204bb385732ec691183e7b
출처 데이터셋
uspto-grants-2014_01
특허 번호
US08633212B2

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