Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxyacetone → 2-Propanone, 1-((methylsulfonyl)oxy)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxyacetone | HCID 8299 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 2-Propanone, 1-((methylsulfonyl)oxy)- | HCID 146754 | — |
반응 단계
Thirty-seven (37) mg of hydroxyacetone was dissolved in 2 ml of chloroform, and to which 0.078 ml of methanesulfonyl chloride was added. After stirring the reaction liquid at room temperature for 30 minutes, saturated aqueous sodium bicarbonate solution was added and extracted with chloroform. The extract was dried over anhydrous sodium sulfate and concentrated to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06699880B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-ae0dc196daec479296ba40aa26395f87 |
| 출처 메모 | uspto-grants-2004_03 |