Hydroxyacetone → 2-Propanone, 1-((methylsulfonyl)oxy)-

HRID 47531

반응식

HRID 47531 반응식
[OH:1][CH2:2][C:3](=[O:5])[CH3:4].[CH3:6][S:7](Cl)(=[O:9])=[O:8].C(=O)(O)[O-].[Na+]>C(Cl)(Cl)Cl>[CH3:6][S:7]([O:1][CH2:2][C:3]([CH3:4])=[O:5])(=[O:9])=[O:8]

참가 물질

5

반응물 3

HCID 8299HydroxyacetoneHCID 31297Methanesulfonyl chlorideHCID 516892Sodium Bicarbonate

생성물 1

HCID 1467542-Propanone, 1-((methylsulfonyl)oxy)-

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

Thirty-seven (37) mg of hydroxyacetone was dissolved in 2 ml of chloroform, and to which 0.078 ml of methanesulfonyl chloride was added. After stirring the reaction liquid at room temperature for 30 minutes, saturated aqueous sodium bicarbonate solution was added and extracted with chloroform. The extract was dried over anhydrous sodium sulfate and concentrated to provide the title compound.

후처리

  1. customthe reaction liquid at room temperature for 30 minutes
  2. extractionextracted with chloroform
  3. dry with materialThe extract was dried over anhydrous sodium sulfate
  4. concentrationconcentrated

출처 및 근거

ORD 기록
ord-ae0dc196daec479296ba40aa26395f87
출처 데이터셋
uspto-grants-2004_03
특허 번호
US06699880B1

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